捲對捲滾輪壓印應用於金屬抗腐蝕之研究

呂明桀

doi:10.6840/cycu201700747

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卷对卷滚轮压印应用於金属抗腐蚀之研究

A study of roll to roll imprinting applied to corrosion protection of metal

吕明桀 , 硕士　　导师：李有璋　　

繁体中文 DOI： 10.6840/cycu201700747

抗腐蚀；卷对卷；奈米压印； anti-corrosion ； roll to roll ； nanoimprinting

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摘要 │ 参考文献 (21) │ 国际计量

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In order to enhance the corrosion resistance of metals, many methods have been proposed, in which the insulation layer coating on the surface of metal is the most popular method to isolate the metal from corrosive media contact. In this study, roll to roll (R2R) equipment was used to imprint the micro/nano structure on the surface of metal  to lead to  hydrophobic effect on the surface, and thereby enhancing the ability of corrosion.
The conventional optical lithography, colloidal lithography and dry etching process were employed to fabricate silicon molds with micro/nano structure, Polydimethylsiloxane (PDMS) soft molds were duplicated from the silicon mode as a embossed template. UV-assisted R2R imprinting method was introduced to transfer the structure from soft mold to the surface of cold-rolled steel. Contact angles were measured to define the hydrophobicity of the surface with/without imprinting structures. The results showed that contact angle of the surface with micro/nano hierarchical structure is 131° which is higher than the angles with micro structure and without imprinting structure. The electrochemical experimental methods was used to characterize the corrosion properties. The ccorrosion potential of steels without any protection and with micro/nano hierarchical are -913.0 mV and -515.7, respectively. The results show that the polymer coating with hydrophobicity effect can effectively improve the corrosion resistance.

参考文献 ( 21 ) 〈TOP〉

[2] Y. N. Singhbabua, B. Sivakumara, J. K. Singhb, H. Bapari, A. K. Pramanick and Ranjan K. Sahu, “Efficient Anti-corrosive Coating of Cold-rolled Steel in Seawater Environment using Oil-based Graphene oxide Ink,” Nanoscale, Vol. 00, pp. 3, 2013.
连结：
[3] K. C. Chang, W. F. Ji, M. C. Lai, Y. R. Hsiao, C. H. Hsu, T. L. Chuang, Y. Wei, J. M. Yeh and W. R. Liu, “Synergistic effects of hydrophobicity and gas barrier properties on the anticorrosion property of PMMA nanocomposite coatings embedded with graphene nanosheets,” Polym. Chem., Vol. 5, pp. 1049, 2014.
连结：
[4] Y. H. Wu, W. J Zhao, W. R Wang and W. J. Sui, “Fabricating binary anti-corrosion structures containing superhydrophobic surfaces and sturdy barrier layers for Al alloys,” RSC Adv., Vol. 6, pp. 5100, 2016.
连结：
[5] P. Wang, D. Zhang , R. Qiu, J. J Wua and Y. Wan, “Super-hydrophobic film prepared on zinc and its effect on corrosion in simulated marine atmosphere, ” Corrosion Science, Vol. 69, pp. 23, 2013.
连结：
[6] M. D. Austin, H. X Ge, W. Wu, M. T. Li, Z. N. Yu, D. Wasserman, S. A. Lyon, and Stephen Y. Chou, “Fabrication of 5 nm linewidth and 14 nm pitch features by nanoimprint lithography, ” Appl. Phys. Lett., Vol. 84, pp. 5299, 2004.
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引用含有DOI的文献

DOI可强化引用精确性、增强学术圈连结，并给予使用者跨平台的良好使用经验，目前在全世界已有超过五千万个对象申请DOI。 如想对DOI的使用与概念有进一步了解，请参考 （ ） 。

DOI可强化引用精确性、增强学术圈连结，并给予使用者跨平台的良好使用经验，目前在全世界已有超过五千万个对象申请DOI。如想对DOI的使用与概念有进一步了解，请参考（）。