奈米碳管薄膜表面改質之製備與應用及其特性分析

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奈米碳管薄膜表面改质之制备与应用及其特性分析

Study on the Preparation and Characterization of Surface Treatment on Transparent Carbon Nanotubes Thin films

廖宏伦 , 硕士　　导师：王本诚　　

英文

奈米碳管；官能基化；共轭高分子；拉曼；叠氮苯氨；分散性； carbon nanotubes ； functionalized ； conjugated polymer ； Raman ； azidoaniline ； dispersibility

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摘要 │ 参考文献 (44) │ 国际计量

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Abstract
This study is working on the two-parts modification of carbon nanotubes(CNTs). (I) Non-covalent (II) Covalent modification 
(I) Pyrene derivatives attach to the surface of CNTs via physisorption, which is the result of a π-π stacking interaction between the pyrene moiety and the CNTs sidewall. We present a simple self-assembly technique to fabricate robust CNTs thin films on glass surface. By employing a cross-linking reagent such as DIC, between the CNT-pyrene complex and the APTES-modified glass substrate with amino groups, it leads to the formation of a strong bonding between CNTs thin films and glass substrate. Characterization by AFM and SEM reveal the morphology of the thin films. The best RMS roughness of our sample is 21.3 nm, which has significant difference compared to the one without APTES-treatment (211nm). We also used water jet to test the interfacial adhesion of the sample and found that the films treated with APTES were robust. Our results on smooth and robust CNTs thin films that show promising potential in industrial applications.
(II) We obtained sidewall functionalized CNTs after radical reacted with 4-azidoaniline hydrochloride by UV source. Modified CNTs were prepared by in situ oxidative polymerization with three different monomers. It was found that the dispersion stability of modified CNTs were significantly improved compared to those of the raw SWCNTs. We used FTIR, XPS and Raman spectra to explain the bonding and quality of modified CNTs. Characterized by TGA and four-point probe to discuss the thermal and electrical properties of modified CNTs.

参考文献 ( 44 ) 〈TOP〉

[1] S. Iijima, "Helical Microtubules of Graphitic Carbon," Nature, vol. 354, pp. 56-58, Nov 7 1991.
连结：
[3] B. E. Kilbride, J. N. Coleman, J. Fraysse, P. Fournet, M. Cadek, A. Drury, et al., "Experimental observation of scaling laws for alternating current and direct current conductivity in polymer-carbon nanotube composite thin films," Journal of Applied Physics, vol. 92, pp. 4024-4030, Oct 1 2002.
连结：
[4] J. K. W. Sandler, J. E. Kirk, I. A. Kinloch, M. S. P. Shaffer, and A. H. Windle, "Ultra-low electrical percolation threshold in carbon-nanotube-epoxy composites," Polymer, vol. 44, pp. 5893-5899, Sep 2003.
连结：
[6] C. Y. Wei, D. Srivastava, and K. J. Cho, "Thermal expansion and diffusion coefficients of carbon nanotube-polymer composites," Nano Letters, vol. 2, pp. 647-650, Jun 2002.
连结：
[7] C. L. Cheung, J. H. Hafner, and C. M. Lieber, "Carbon nanotube atomic force microscopy tips: Direct growth by chemical vapor deposition and application to high-resolution imaging," Proceedings of the National Academy of Sciences of the United States of America, vol. 97, pp. 3809-3813, Apr 11 2000.
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使用DOI作为永久连结

引用含有DOI的文献

DOI可强化引用精确性、增强学术圈连结，并给予使用者跨平台的良好使用经验，目前在全世界已有超过五千万个对象申请DOI。 如想对DOI的使用与概念有进一步了解，请参考 （ ） 。

DOI可强化引用精确性、增强学术圈连结，并给予使用者跨平台的良好使用经验，目前在全世界已有超过五千万个对象申请DOI。如想对DOI的使用与概念有进一步了解，请参考（）。